机构地区: 黑龙江大学化学化工与材料学院
出 处: 《应用化学》 2003年第8期794-796,共3页
摘 要: The α Fe 2 O 3 sol was prepared by a sol gel method from FeCl 3 ·6H 2 O. Thin nano particulate films of the α Fe 2 O 3 were deposited on glass substrate by dip coating sol gel technique. The structure and morphology of the thin films were characterized by XRD, UV Vis and AFM analysis methods. The XRD results revealed that the nano crystal with (104) preferential orientation has been formed on glass substrate. The UV Vis spectra showed that the nano particulate films obtained from Fe 2 O 3 aqueous colloidal sols are well transferred to glass substrate at dip coating rate of 80 mm/min. The α Fe 2 O 3 particles are ellipsoidal shaped, with particle size of about 5~7 nm. The multilayer films exhibited high sensitivity to ethanol vapor at room temperature. The α Fe 2 O 3 sol was prepared by a sol gel method from FeCl 3 ·6H 2 O. Thin nano particulate films of the α Fe 2 O 3 were deposited on glass substrate by dip coating sol gel technique. The structure and morphology of the thin films were characterized by XRD, UV Vis and AFM analysis methods. The XRD results revealed that the nano crystal with (104) preferential orientation has been formed on glass substrate. The UV Vis spectra showed that the nano particulate films obtained from Fe 2 O 3 aqueous colloidal sols are well transferred to glass substrate at dip coating rate of 80 mm/min. The α Fe 2 O 3 particles are ellipsoidal shaped, with particle size of about 5~7 nm. The multilayer films exhibited high sensitivity to ethanol vapor at room temperature.