作　　者： ; ; ; ; ;

机构地区： 中山大学化学与化学工程学院

出　　处： 《应用化学》 2003年第1期80-82,共3页

摘　　要： Title thioureas have been synthesized by reaction of substituted phenylamines with 1,4- or 1,3-benzenedicarbonyl chloride and ammonium thiocyanate by solid-liquid phase transfer catalysis using polyethylene glycol-400(PEG-400) as a catalyst in yield of 80%～96%. The compounds were characterized and identified by elemental analysis, IR and 1H NMR. Title thioureas have been synthesized by reaction of substituted phenylamines with 1,4- or 1,3-benzenedicarbonyl chloride and ammonium thiocyanate by solid-liquid phase transfer catalysis using polyethylene glycol-400(PEG-400) as a catalyst in yield of 80%～96%. The compounds were characterized and identified by elemental analysis, IR and 1H NMR.

关 键 词： 相转移催化法 合成 苯二甲酰基硫脲衍生物

领　　域： [理学] [理学] [理学] [理学]