作　　者： ; ; ; ; ;

机构地区： 辽宁大学化学院

出　　处： 《无机化学学报》 2009年第3期560-562,共3页

摘　　要： A three-dimensional two-fold inorganic-organic hybrid complex:[Cd(C5H3O2)2(H2O)]n(1),was synthesized under mild hydrothermal condition,and the X-ray crystal structure analysis was used to determined the structure.The complex crystallizes in the orthorhombic space group Pbca,with a=1.147 6(2) nm,b=1.211 1(2) nm,c=1.750 3(4) nm,V=2.432 6(8) nm3,Z=8,R1=0.032 3,wR2=0.134 3. A three-dimensional two-fold inorganic-organic hybrid complex： [Cd（C5H3O2）2（H2O）], （1）, was synthesized under mild hydrothermal condition, and the X-ray crystal structure analysis was used to determined the structure. The complex crystallizes in the orthorhombic space group Pbca, with a=1.147 6（2） nm, b=1.211 1 （2） nm, c=1.750 3（4） nm, V=2.4326（8） nm^3, Z=8, R1=0.032 3, wR^2=0.1343. CCDC： 714446.

关 键 词： 二重互穿 三维 水热合成 晶体结构

领　　域： [理学] [理学]