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猴头菌寡糖的分离及其结构确定
Separation and Structural Identification of Hericium Erinaceur Oligosaccharide

作  者: ; ; ; ; ; ;

机构地区: 吉林省中医中药研究所

出  处: 《高等学校化学学报》 2007年第7期1313-1315,共3页

摘  要: It has been reported that the polysaccharide is the main active constituent of Hericium erinaceur.A series of oligosaccharide(mixtures of disaccharide and heptasaccharide of Hericium erinaceur) were separated from Hericium erinaceur by empty-fibrin filtration.Disaccharide and trisaccharide were purified via HPLC with NH2 column.Component sugars and glycosidic linkage ways were analysed via GC and GC-MS.Electrospray ionization tandem mass spectrometry(MSn) was used for the oligosaccharides structure study and the result shows that the disaccharide has two kind of structural styles and trisaccharide has one kind of structural style. It has been reported that the polysaccharide is the main active constituent of Hericium erinaceur. A series of oligosaccharide( mixtures of disaccharide and heptasaccharide of Hericium erinaceur) were separated from Hericium erinaceur by empty-fibrin filtration. Disaccharide and trisaccharide were purified via HPLC with NH2 column. Component sugars and glycosidic linkage ways were analysed via GC and GC-MS. Electrospray ionization tandem mass spectrometry ( MSn ) was used for the oligosaccharides structure study and the result shows that the disaccharide has two kind of structural styles and trisaccharide has one kind of structural style.

关 键 词: 猴头菌浸膏 寡糖 电喷雾多级串联质谱

领  域: [理学] [理学] [理学] [理学]

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