作　　者： ; ; (曹钢）; (于晓东）;

机构地区： 华东理工大学化学与分子工程学院工业催化研究所

出　　处： 《光谱学与光谱分析》 2007年第5期1032-1035,共4页

摘　　要： 在100,250和1000mL高压釜静态成功合成MCM-22分子筛的基础上,在2,5和200L高压釜中进行了MCM-22分子筛的动态合成试验,对合成的样品用XRD等技术进行了表征。结果表明,在静态和动态条件下合成的样品,全部为纯相MCM-22分子筛,且结晶度较高,从100mL到200L的放大试验是成功的。 On the basis of MCM-22 zeolite synthesis at the static condition in 100 mL lined PTFE autoclave, 250 and 1 000 mL stainless steel autoclave respectively, the synthesis of MCM-22 zeolite was studied at the rotating condition in 2, 5 and 200 L autoclave respectively. The samples as-synthesized and calcined were characterized by means of XRD and so on. The results show that all the synthesized samples are the pure MCM-22 zeolites, and their crystallinities were high, and MCM-22 zeolite can be synthesized successfully at the rotating condition in 200 L stainless steel autoclave.

关 键 词： 分子筛 水热合成 放大实验 测试

领　　域： [化学工程] [化学工程]