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表面修饰In纳米微粒的声化学法制备及结构表征
Preparation and Characteration of Surface Modified Indium Nanoparticles by Sonochemistry

作  者: ; ; ; ; (李志伟); (党鸿辛);

机构地区: 中国科学院兰州化学物理研究所固体润滑国家重点实验室

出  处: 《无机化学学报》 2005年第8期1261-1264,共4页

摘  要: Surface modified indium nanoparticles were prepared by a simple and rapid process from bulk indium via ultrasound dispersion. The morphology and structure of synthesized nanoparticles were characterized by TEM, XRD, XPS and FTIR. The results show that the morphology of indium nanoparticles is spherical and the structure of indium nanoparticles is the tetragonal phase. The surface of indium nanoparticles was coated by 2 ethyl hexanoic acid, which could almost hold back oxidation of the indium nanoparticles. In addition, the tribological property of indium nanoparticles as additives in oil was evaluated on a four-ball tester and the results show that indium nanoparticles exhibit good performance in wear. Surface modified indium nanoparticles were prepared by a simple and rapid process from bulk indium via ultrasound dispersion. The morphology and structure of synthesized nanoparticles were characterized by TEM, XRD, XPS and MR. The results show that the morphology of indium nanoparticles is spherical and the structure of indium nanoparticles is the tetragonal phase. The surface of indium nanoparticles was coated by 2 ethyl hexanoic acid, which could almost hold back oxidation of the indium nanoparticles. In addition, the tribological property of indium nanoparticles as additives in oil was evaluated on a four-ball tester and the results show that indium nanoparticles exhibit good performance in wear.

关 键 词: 纳米微粒 声化学 制备 摩擦学

领  域: [理学] [理学] [理学] [理学]

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