机构地区: 国防科学技术大学航天与材料工程学院新型陶瓷纤维及其复合材料国家重点实验室
出 处: 《化工新型材料》 2005年第4期40-43,共4页
摘 要: 本文研究了聚铁碳硅烷的合成,探索了裂解温度、反应温度、二茂铁等因素对合成聚铁碳硅烷(PFCS)工艺的影响;元素分析、红外光谱、氢谱分析表明:铁被引入到聚铁碳硅烷(PFCS)中,PFCS与聚碳硅烷(PCS)的结构相似。 In this paper synthesis of polyferrocarbosilane(PFCS) was studied, synthesis techniques including reaction temperature, pyrolysis temperature and ferrocene were investigated. Iron was inducted to the PFCS and the structure of polyferrocarbosilane resembles polycarbosilane′s, which were characterized by elements analysis,FT-IR and 1H-NMR.