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低温液相制备金红石型TiO_2纳米晶须
Synthesis of Rutile TiO_2 Nanowhiskers by Liquid Phase Method at Low Temperature

作  者: ; ; ; ;

机构地区: 河北师范大学化学与材料科学学院

出  处: 《高等学校化学学报》 2004年第11期1996-1997,共2页

摘  要: By using a simply liquid phase method at a low temperature, rutile TiO 2 nanowhiskers were successfully prepared from TiCl 4 aqueous solution at 70 ℃ after aging for 11 d. The obtained TiO 2 nanowhiskers were characterized by means of TEM,HRTEM and XRD. The results show that the nanowhiskers are rutile crystals growing along c-axis direction with a length of 100150 nm and a diameter 68 nm. The simple fabrication method of TiO 2 nanowhiskers will promote practical application of 1D TiO 2. By using a simply liquid phase method at a low temperature, rutile TiO 2 nanowhiskers were successfully prepared from TiCl 4 aqueous solution at 70 ℃ after aging for 11 d. The obtained TiO 2 nanowhiskers were characterized by means of TEM,HRTEM and XRD. The results show that the nanowhiskers are rutile crystals growing along c-axis direction with a length of 100_150 nm and a diameter 6_8 nm. The simple fabrication method of TiO 2 nanowhiskers will promote practical application of 1D TiO 2.

关 键 词: 纳米晶须 液相制备

领  域: [理学] [理学]

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